Low Temperature Solution Route Approaches to Oxide Functional Nanoscale Materials

The route to functional graphene oxide.

We report on an easy-to-use, successful, and reproducible route to synthesize functionalized graphite oxide (GO) and its conversion to graphene-like materials through chemical or thermal reduction of GO. Graphite oxide containing hydroxyl, epoxy, carbonyl, and carboxyl groups loses mainly hydroxyl and epoxy groups during reduction, whereas carboxyl species remain untouched. The interaction of f...

Chemical precipitation and characterization of multicomponent Perovskite Oxide nanoparticles – possible cathode materials for low temperature solid Oxide fuel cell

A set of multicomponent perovskite oxide nanoparticles based on La1-xSrxCo1-yFeyO3-δ(LSCF) were prepared by a simple chemical precipitation method for application in low temperature solid oxide fuel cells (LT-SOFC) as cathode materials.  The precursor materials used in this synthesis were lanthanum nitrate hexahydrate [La(NO3)<su...

Chemical precipitation and characterization of multicomponent Perovskite Oxide nanoparticles – possible cathode materials for low temperature solid Oxide fuel cell

A set of multicomponent perovskite oxide nanoparticles based on La1-xSrxCo1-yFeyO3-δ(LSCF) were prepared by a simple chemical precipitation method for application in low temperature solid oxide fuel cells (LT-SOFC) as cathode materials.  The precursor materials used in this synthesis were lanthanum nitrate hexahydrate [La(NO3)<su...

Solution design for Low Fluorine Trifluoroacetate route to YBa2Cu3O7

Nanocrystal seeding: A low temperature route to polycrystalline Si films

A novel method is presented for growth of polycrystalline silicon films on amorphous substrates at temperatures of 540-575 “C. Grain nucleation and grain growth are performed in two steps, using Si nanocrystals as nuclei (“sceds’“,L The nanocrystal seeds are produced by excimer laser photolysis of disilane in a room temperature flow cell. Film (grain) growth occurs epitaxially on the seeds in a...